SYNTHESES OF N- METHYL- ¹⁴C BENZYL AMINE AND N- METHYL- ¹⁴C BENZYL NITROSAMINE

SYNTHESES OF N- METHYL- 14 C BENZYL AMINE AND N- METHYL- 14 C BENZYL NITROSAMINE 1 first-author 1 1 1 1 Shanghai Institute of Nuclear Research, Academia Sinica, Shanghai 201800 Shanghai Institute of Nuclear Research, Academia Sinica, Shanghai 201800 The syntheses of N - Methyl- 14 C benzyl amine and N - Methyl- 14 C benzyl nitrosamine are reported. Specific activities were approximately 920 MBq/mmol. Chemical and radiochemical purity checked by HPLC were more than 95%. N - Methyl- 14 C benzyl amine N - Methyl- 14 benzyl nitrosamine Trifluoroacetamide 14 C - Labelled compounds REFERENCES E.J. Bourne et al ., J. Chem. Soc. , ( 1952 ), 4041 . J. Chem. Soc. A. Taurog et al ., J. Am. Chem. Soc. , 75 ( 1953 ), 3473 . J. Am. Chem. Soc. J. Eric Nordlander et al ., Tetrahedron Letters. , 50 ( 1978 ), 4987 . Tetrahedron Letters. R.A.W. Johnstone et al ., J. Chem. Soc. , C ( 1969 ), 2223 . J. Chem. Soc. A.P. King and C.G. Krespan , J. Org. Chem. , 39 ( 1974 ), 1315 . J. Org. Chem. 1990-08-01 2021-02-05 1990 Nuclear Science and Techniques 3 1