Data-collection system for high-throughput X-ray absorption fine structure measurements

Rui-You Lu; Qian Gao; Song-Qi Gu; Ya-Yun Yang; Rui Si

doi:10.1007/s41365-016-0084-8

Your Location：

Home >

Browse articles >

Data-collection system for high-throughput X-ray absorption fine structure measurements

LOW ENERGY ACCELERATOR, RAY AND APPLICATIONS | Updated：2021-02-23

- Data-collection system for high-throughput X-ray absorption fine structure measurements
- Nuclear Science and Techniques Vol. 27, Issue 4, Article number: 82(2016)
- Affiliations：
  
  1.Shanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai 201204, China
  2.University of Chinese Academy of Sciences, Beijing 100049, China
- Author bio：
  
  Corresponding author: E-mail: gaoqian@sinap.ac.cn
- Funds：
- DOI：10.1007/s41365-016-0084-8
  CLC：
Scan for full text
Rui-You Lu, Qian Gao, Song-Qi Gu, et al. Data-collection system for high-throughput X-ray absorption fine structure measurements. [J]. Nuclear Science and Techniques 27(4):82(2016)
DOI：

Rui-You Lu, Qian Gao, Song-Qi Gu, et al. Data-collection system for high-throughput X-ray absorption fine structure measurements. [J]. Nuclear Science and Techniques 27(4):82(2016) DOI： 10.1007/s41365-016-0084-8.

摘要

Abstract

A new X-ray absorption fine structure (XAFS) data-collection system based on the Experimental Physics and Industrial Control System software environment has been established at the BL14W1 beamline of the Shanghai Synchrotron Radiation Facility. The system provides for automatic sequential analysis of multiple samples for continuous high-throughput (HT) measurements. Specifically, 8 sample pellets are loaded into an alumina holder, and a high-precision two-dimensional translation stage is programmed to switch these samples automatically for collecting the XAFS spectrum of each sample in sequence. Experimenters implement HT measurements via a graphical user interface developed with Control System Studio. Finally, the successful operation of the HT XAFS system is demonstrated by running experiments on two groups of copper-ceria catalysts, each of which contains 8 different powder samples.

关键词

Keywords

X-ray absorption fine structureHigh throughputControl System StudioExperimental Physics and Industrial Control SystemGraphical User InterfaceData collection.

references

Hoogenboom R, Wiesbrock F, Leenen M A, et al. Accelerating the living polymerization of 2-Nonyl-2-oxazoline by implementing a microwave synthesizer into a high-throughput experimentation workflow. J Comb Chem, 2005, 7: 10-13. DOI: 10.1021/cc049846fhttp://doi.org/10.1021/cc049846f

Potyrailo R A, Morris W J, Wroczynski R J, et al. Resonant multisensor system for high-throughput determinations of solvent/polymer interactions. J Comb Chem, 2004, 9: 869-873. DOI: 10.1021/cc049925rhttp://doi.org/10.1021/cc049925r

Potyrailo R A, Wroczynski R J, Lemmon J P, et al. Fluorescence spectroscopy and multivariate spectral descriptor Analysis for high-throughput multiparameter optimization of polymerization conditions of combinatorial 96-microreactor arrays. J Comb Chem, 2003, 5: 8-17. DOI: 10.1021/cc020062ghttp://doi.org/10.1021/cc020062g

Venimadhav A, Yates K A, Blamire M G, Scanning raman spectroscopy for characterizing compositionally spread films. J Comb Chem, 2005, 7: 85-89. DOI: 10.1021/cc049927bhttp://doi.org/10.1021/cc049927b

Leugers A, Neithamer D R, Sun L S, et al. High-throughput analysis in catalysis research using novel approaches to transmission infrared spectroscopy. J Comb Chem, 2003, 5: 238-244. DOI: 10.1021/cc0200944http://doi.org/10.1021/cc0200944

Miller T C, Mann G, Havrilla G J, et al. Micro-X-ray fluorescence as a general high-throughput screening method for catalyst discovery and small molecule recognition. J Comb. Chem, 2003, 5: 245-252. DOI: 10.1021/cc020102ghttp://doi.org/10.1021/cc020102g

Taniguchi M M, Farrer R A, Fourkas J T. In situ observation of molecular diffusion in solid supports using two-photon fluorescence microscopy. J Comb. Chem, 2005, 7: 54-57. DOI: 10.1021/bp0257291http://doi.org/10.1021/bp0257291

Gibbs P R, Uehara C S, Nguyen P T, et al. Imaging polarimetry for high throughput chiral screening. Biotechnol Progr, 2003, 19: 1329-1334. DOI: 10.1021/bp0257291http://doi.org/10.1021/bp0257291

Kautz R A, Goetzinger W K, Karger B L. High-throughput microcoil NMR of compound libraries using zero-dispersion segmented flow analysis. J Comb Chem, 2005, 7: 14-20. DOI: 10.1016/j.jpba.2004.11.007http://doi.org/10.1016/j.jpba.2004.11.007

Reibenspies J H, Bhuvanesh N S. Combinatorial screening employing nylon loops and micro-X-ray powder diffraction. J Pharmaceut Biomed, 2005, 37: 611-614. DOI: 10.1016/j.jpba.2004.11.007http://doi.org/10.1016/j.jpba.2004.11.007

Shi W X, Zhan C Y, Ignatov A, et al. Metalloproteomics: High-throughput structural and functional annotation of proteins in structural genomics. Structure, 2005, 13: 1473-1486. DOI: 10.1016/j.str.2005.07.014http://doi.org/10.1016/j.str.2005.07.014

Bingel-Erlenmeyer R, Olieric V, Grimshaw, J P A, et al. SLS Crystallization Platform at Beamline X06DA—A Fully Automated Pipeline Enabling in Situ X-ray Diffraction Screening. Cryst Growth Des, 2011, 11: 916-923. DOI: 10.1021/cg101375jhttp://doi.org/10.1021/cg101375j

Tsapatsaris N, Beesley A M, Weiher N, et al. X-Ray Absorption Fine Structure-XAFS13. Melville (USA): Amer Inst Physics, 2007, 597-599.

Yu H S, Wei X J, Li J, et al. The XAFS beamline of SSRF. Nucl Sci Tech, 2015, 26: 050102. DOI: 10.13538/j.1001-8042/nst.25.020103http://doi.org/10.13538/j.1001-8042/nst.25.020103

EPICS Home Page. http://www.aps.anl.gov/epics/http://www.aps.anl.gov/epics/

Hu Z, Mi Q R, Zhen L F, et al. EPICS data archiver at SSRF beamlines. Nucl Sci Tech, 2014, 25: 20103. DOI: 10.13538/j.1001-8042/nst.25.020103http://doi.org/10.13538/j.1001-8042/nst.25.020103

Dalesio L R, Kraimer M R, Kozubal A J. EPICS architecture, in Proceedings of International Conference on Accelerator and Large Experimental Physics Control Systems, Tsukuba, Japan,602-611, Oct. 1991.

Jia W H, Ma S W, Zheng L F. The control system for water-cooled DCMS in SSRF. Nucl Sci Tech, 2015, 26: 020103. DOI: 10.13538/j.1001-8042/nst.26.020103http://doi.org/10.13538/j.1001-8042/nst.26.020103

Jacky J. EPICS-based control system for a radiation therapy machine, 14th International Conference on Accelerator & Large Experimental Physics Control Systems, San Francisco, USA, 933-925, Oct. 2013.

StreamDevice Home Page. http://epics.web.psi.ch/software/streamdevice/http://epics.web.psi.ch/software/streamdevice/

Mooney T. The sscan record for sscan module R2.10. http://www.aps.anl.gov/bcda/synApps/sscan/sscanRecord.htmlhttp://www.aps.anl.gov/bcda/synApps/sscan/sscanRecord.html

Mooney T. SynApps sscan module. http://www.aps.anl.gov/aod/bcda/synApps/sscan.htmlhttp://www.aps.anl.gov/aod/bcda/synApps/sscan.html

Kasemir K, Carcassi G. Control System Studio Guide http://cs-studio.sourceforge.net/docbookhttp://cs-studio.sourceforge.net/docbook.

Views

Downloads

CSCD

Alert me when the article has been cited

Submit

Tools

Publicity Resources

Novel design of a personnel safety system for Hefei Light Source-II

Soller slits automatic focusing method for multi-element fluorescence detector

The XAFS beamline of SSRF

The new control system of HLS linac and transport line

Related Author

No data

Related Institution

National Synchrotron Radiation Laboratory, University of Science and Technology of China

National Synchrotron Radiation Lab., University of Science and Technology of China

Address：Editorial Office of NST, 2019 Jialuo Road, Jiading, Shanghai 201800, China Postal code：201800
Email：nst@sinap.ac.cn
Technical support is provided by Beijing Founder electronics co., LTD 沪ICP备05005479号-1 京公网安备11010802024621
It is recommended to read the content of this site in Chrome&IE9+. Please switch to extreme mode in browser 360.
Cookies We use cookies to help provide and enhance our service and tailor content. By continuing, you agree to the use of cookies.

⁰