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Ultrasonic-assisted synthesis and strepavidin conjugation of amino-magnetic nanoparticles

MISCELLANEOUS

Ultrasonic-assisted synthesis and strepavidin conjugation of amino-magnetic nanoparticles

LIU Li
JIAO Qinghua
PENG Cheng
HE Shijiang
WANG Lihua
Nuclear Science and TechniquesVol.19, No.6pp.370-375Published in print 20 Dec 2008
31000

MNPs are widely used in biotechnology, magnetic resonance imaging, catalysis and other areas. In this paper, we propose a simple, quick, inexpensive and efficient way to prepare amino-MNPs with sonication-assisted process. The amino-MNPs prepared by hydrolyzing TEOS and APS were characterized by SEM, TEM and FTIR. Conjugation of SA and amino-MNPs was also studied. The biotin bound capacity of prepared SA coated amino-MNPs was 1.824 nmol/mg, which well meet the need of biological application.

Magnetic nanoparticlesStrepavidinBiotin bound capacitySonication-assisted surface treatment
References
[1] Lu A, Salabas E, Schuth F. Angew Chem Int Ed, 2007, 46(8): 1222-1244.
[2] Salgueirino-Maceira V, Correa-Duarte M. Adv Mater, 2007, 19(23): 4131-4144.
[3] Gupta A, Gupta M. Biomaterials, 2005. 26(18): 3995-4021.
[4] Tedesco A, Oliveira D, Lacava G. J Magn Magn Mater, 2004. 272-276: 2404-2405.
[5] Tedesco A, Oliveira D, Lacava Z, et al. J Appl Phys, 2003, 93(10): 6704-6706.
[6] Iijima M, Yonemochi Y, Tsukada M, et al. J Colloid Interface Sci, 2006, 298(1): 202-208.
[7] Kobayashi Y, Horie M, Konno M, et al. J Phys Chem B, 2003, 107(30): 7420-7425.
[8] Ma M, Zhang Y, Yu W, et al. Colloid Surface A-Physicochemical and Engineering Aspects, 2003, 212(2-3): 219-226.
[9] Del Campo A, Sen T, Lellouche J, et al. J Magn Magn Mater, 2005, 293(1): 33-40.
[10] Hamley I. Angew Chem Int Ed, 2003, 42(15): 1692-1712.
[11] Tepper T, Ilievski F, Ross C, et al. J Appl Phys, 2003, 93(10): 6948-6950.
[12] Chen Q, Boothroyd C, Tan G, et al. Langmuir, 2008, 24(3): 650-653.
[13] Hong J, Gong P, Yu J, et al. J Mol Catal B-Enzym, 2006, 42(3-4): 99-105.
[14] Gao F, Pan B, Zheng W, et al. J Magn Magn Mater, 2005, 293(1): 48-54.
[15] Ulman A. Chem Rev, 1996, 96(4): 1533-1554.
[16] Tartaj P, Gonzalez-Carreno T, Serna C, et al. Adv Mater, 2001, 13(21): 1620-1624.
[17] Santra S, Tapec R, Theodoropoulou N, et al. Langmuir, 2001, 17(10): 2900-2906.
[18] Liu X, Ma Z, Xing J. et al. J Magn Magn Mater, 2004, 270(1-2): 1-6.
[19] Khan A, Luckham P, Manimaaran S. J Mater Chem, 1997, 7(9): 1849-1853.
[20] Suslick K, Fang M, Hyeon T. J Am Chem Soc, 1996, 118(47): 11960-11961.
[21] Hyeon T, Fang M, Suslick K. J Am Chem Soc, 1996, 118(23): 5492-5493.
[22] Chen Q, Boothroyd C, Tan G, et al. Langmuir, 2008, 24(3): 650-653.
[23] Blanco E, Luis L, Rocío P, et al. Appl Organomet Chem, 1999, 13(5): 399-418.
[24] Zhang Z, Zhu H, Tang Y, et al. Sci China Series B-Chemistry, 2007, 50(1): 127-134.