Advances in insertion device technology, top-up operation and superconducting RF cavities make it possible to generate high brightness X-ray with intermediate energy light sources, which leads a new trend in designing and constructing third generation light sources around the world. The development status and the remarkable technical features of intermediate energy light sources are reviewed, and the main SSRF properties are described in this paper.
Vol.14, No.1
Select issueYearIssue
2003
1
SYNCHROTRON TECHNOLOGY AND APPLICATIONS
Research article 01 Feb 2003
ZHAO Zhen-Tang
keyword:Light source;Storage ring;Insertion devices;Beam stability;Superconducting RF;
Research article 01 Feb 2003
M. BENFATTO,WU Zi-Yu
In this paper we present the state of the art of the theoretical background needed for analyzing x-ray absorption spectra in the whole energy range. The multiple-scattering (MS) theory is presented in detail with some applications on real systems. We also describe recent progress in performing geometrical fitting of the XANES (X-ray absorption near-edge structure) energy region and beyond using a full multiple-scattering approach.
keyword:X-ray absorption spectroscopy;X-ray absorption near-edge structure;Multiple-scattering theory;
Research article 01 Feb 2003
SHENG Shu-Gang,LIN Guo-Qiang,GU Qiang,LI De-Ming
A 100 kV triode-electron-gun has been designed and manufactured for the Linac of Shanghai Synchrotron Radiation Facility (SSRF). In this paper the performance of the gun and some key components are described.
keyword:Thermionic gun;EGUN;
Research article 01 Feb 2003
CHENG Wei-xing,LIU De-Kang
The newly developed Digital Beam Position Monitor (DBPM) system is introduced. The DBPM system differs with the conventional beam position monitor system in the use of DSP chips and the digital signal processing technology. It can be programmed on-line to select operation modes through EPICS control panel, and to measure various parameters of the third generation synchrotron radiation facility. This DBPM system can be used in the pre-injector LINAC, the transfer lines, the booster synchrotron and the storage ring. The electronic parameters of the DBPM system itself have been measured also.
keyword:DBPM;DSP;VME64x;
Research article 01 Feb 2003
Didier SÉBILLEAU,WU Zi-Yu
We present here a general overview of electron spectroscopies from a practical point of view. The most frequently used ones are described and the type of structural information they can provide on materials is explained in relation to the physical processes on which they are based. Furthermore, we explore critically and in detail various tools that have been developed to allow a systematic solving of structures by these spectroscopies.
keyword:Electron spectroscopy;Materials characterization;Surface analysis;
NUCLEAR, HEAVY ION AND ATOMIC PHYSICS
Research article 01 Feb 2003
YANG Wei-Fan,PAN Qiang-Yan,MA Tao-Tao,YUAN Shuang-Gui,GUO Jun-Sheng,KONG Deng-ming,QIAO ji-min,LUO Zi-hao,ZHANG Mu-tian,WANG Shu-hong
230Pa was produced through the 232Th(p,3n)230Pa reaction in the irradiated ThO2 powder targets with 35 MeV proton beam. Pa was radiochemically separated from ThO2 and other reaction products, and then thin sources of 230Pa→β−230U were prepared. The polyethylene-terephthalate (lavsan) films were selected as solid track detector searching for the cluster activity of 230U. The gamma activity of 230Pa in the sources was measured using a HPGe detector. The lavsan films were etched in NaOH solution and the etched films were scanned under an optical microscope. The exotic nuclear decay of 230U by emission of 22Ne was observed. A branching ratio relative to α decay was deduced, B =λNe/λα = (1.3±0.8)×10-14 for 22Ne emission from 230U.
keyword:230U;22Ne emission;232Th(p,3n)230Pa reaction;
Research article 01 Feb 2003
HE Ze-Jun,ZHANG Jia-Ju,LONG Jia-Li,JIANG Wei-Zhou
We find that in a chemically equilibrating baryon-rich quark-gluon matter, due to the slow cooling rate, high initial temperature, large gluon density as well as large fusion cross section of gg→cc in the intermediate mass region, the gluon fusion gg→cc provides a dominant contribution to dileptons with intermediate masses, resulting in the significant enhancement of intermediate mass dileptons.
keyword:Relativistic unclear collisions;Chemical non-equilibrium;Dileptons;
LOW ENERGY ACCELERATOR, RAY TECHNOLOGY AND APPLICATIONS
Research article 01 Feb 2003
HUANG Ning-Kang,YANG Bin,XIONG Qi,LIU Yao-Guang
SiC-C films with different content of SiC were deposited with r. f. magnetron sputtering followed by argon ion bombardment. These films were then permeated by hydrogen gas under the pressure of 3.23×107 Pa for 3h at 500K. AES and XPS were used to analyze chemical bonding states of C and Si in the SiC-C films as well as contaminating oxygen before and after hydrogen gas permeation in order to study the effect of hydrogen on them. Related mechanism was discussed in this paper.
keyword:SiC-C films;Hydrogen permeation;XPS;AES;
Research article 01 Feb 2003
ZHENG Li-Ping,JIANG Bing-Yao,LIU Xiang-Huai,LI Dou-Xing
The Monte Carlo simulation with the energetics described by the embedded atom method has been employed to mainly study physical behaviors of boron atoms during relaxation of the Ni3Al-x at.% B grain boundary. During relaxation of impure Ni3Al grain boundaries, we suggest that for different types of impure atoms(Mg, B, Cr and Zr atoms etc.), as the segregating species, they have the different behaviors, but as the inducing species, they have the same behaviors, i.e. they all induce Ni atoms to substitute Al atoms. Calculations show that at the equilibrium, when x(the B bulk concentration) increases from 0.1 to 0.9 , the peak concentration of B increases, correspondently, the peak concentration of Ni maximizes but the valley concentration of Al minimizes, at x = 0.5. The calculations also show the approximate saturation of Ni at the grain boundary at x = 0.5.
keyword:Grain boundary;Segregating species;Inducing species;
RADIOCHEMISTRY, RADIOPHARMACEUTICALS AND NUCLEAR MEDICINE
Research article 01 Feb 2003
DING Shi-Yu,LIN Yan-Song,CHEN Zheng-Ping,JI Shu-Ren,LU Chun-Xiong,ZHOU Xiang,FANG Ping,WU Chun-Ying,WANG Bo-Cheng,XIANG Jing-De
The method to synthesize a high affinity muscarinic receptor antagonist (R,S)I-QNB[(R)-(-)-1-azabicyclo [2,2,2]oct-3-yl-(S)-(+)-α-hydroxy-α-(4-[127I]iodophenyl)-α-phenyl acetate] from 4-nitrobenzophenone with improvement compared to literatures was reported in this article. IR, MS and 1HNMR characterized the final product. (R,S)131I-QNB was prepared using Cu(I) assisted iodine exchange labeling, and showed by TLC that the radiolabeling yield(RLY) was over 80%, and radiochemical purity(RCP) was over 95%. Stability of the labeled compound was also determined. It was found that (R,S)131I-QNB dried by nitrogen blowing can stay at 4-10℃ for a week without change of RCP.
keyword:(R,S)I-QNB;Preparation;131I labeling;Cerebral muscarinic acetylcholine receptors;
Research article 01 Feb 2003
LI Jun-ling,WANG Yong-xian,ZHANG Xiu-li,ZHOU Wei,TIAN Hai-bin,YIN Duan-zhi
N-succinimidyl 4-[18F](fluoromethyl) benzoate for protein labeling was prepared (57%, EOB) in about 30min. Reaction conditions of S18FMB with IgG including pH of solutions, protein concentration, reaction temperature and time were studied. The optimal labeling conditions were: 0.2mg/mL IgG, pH = 7.8-8.5, 25℃, and reaction time 5min.Under these conditions the yield was about 80%. The 18F-labeled protein was purified by size exclusion chromatography.
keyword:S18FMB;IgG;Protein labeling;Size exclusion chromatography;
ADVANCED NUCLEAR INSTRUMENTATION AND DETECTION
Research article 01 Feb 2003
CUI Yi-Min,PAN Wan-Jiang,WU Song-Tao,WAN Yuan-Xi
The HT-7U superconducting Tokamak is a whole superconducting magnetically confined fusion device. The insulating system of its central solenoid coils is critical to its properties. In this paper the forming of the insulating system and the vacuum-pressure-impregnating (VPI) are introduced, and the whole insulating process is verified under the superconducting experiment condition.
keyword:HT-7U;CS;Vacuum pressure impregnation;
Research article 01 Feb 2003
FANG Jin,WENG Pei-De,CHEN Zhuo-Min,CHEN Jing-lin,WANG Fu-tang,HAN Zheng-He
Superconducting TF and PF coils have been measured in SULTAN test facility. Segregated copper strands are included in four NbTi CICC and this is a technical innovation. Two AC losses measurement methods, calorimetric and electromagnetic methods, have been used in the experiments, and a broad frequency range (from 0.05 Hz to 6 Hz) is covered in sample test. The purpose of this experiment was to investigate AC losses of TF and PF CICC conductor including segregated copper and to check the design of PF and TF CICC coated with different resistive barriers (Pb–30Sn-2Sb and Ni plating on NbTi strands).
keyword:cable-in-conduit conductor;Coupling loss time constant;Sn and Ni plated conductor;Contact resistance;
Research article 01 Feb 2003
JING Shi-wei,LIU Lin-mao
The microwave absorption efficiency, which is relevant to magnet field and its distribution, is a major parameter of the microwave ion source (MWIS) for the intense neutron tube. Based on previous work, the relations between microwave absorption efficiency and plasma chamber structure and thickness of the microwave introduction window are studied. The microwave absorption efficiency reaches to 100% when plasma chamber is 100mm long and the window thickness is 30mm. The microwave absorption efficiency as a function of pressure is also presented.
keyword:Microwave ion source;Absorption efficiency;Plasma chamber;
Research article 01 Feb 2003
HUANG Shi-Bin,McNEILL F E,CHETTLE D R
The precision of results obtained from the 109Cd K XRF in vivo measurement system of bone lead for obese subjects with high BMI (body mass index) was poor. The main factor affecting the precision was the distance between tibia and detector. Compared with the standard phantom, a large phantom was used to simulate the obese subject in the measurements at different distances to the detector. The counts of Compton scattering increased highly because of the tissue overlying and surrounding tibia of the obese subject. When the distance between leg and detector was too small, the instrument would produce the distorted x-ray spectra, so that the obtained data were inaccurate. In order to ensure good measurement precision and accuracy, the distance between leg and detector should be maintained at 25 mm during the counting period. Meanwhile, the dead time displayed instantly on the instrument should be controlled to around 30%.
keyword:Measurement distance;X-ray fluorescence;Bone lead;Obese subjects;